ASTM C759-98

Standard Test Methods for Chemical, Mass Spectrometric, Spectrochemical, Nuclear, and Radiochemical Analysis of Nuclear-Grade Plutonium Nitrate Solutions

STANDARD published on 10.2.1998

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The information about the standard:

Designation standards: ASTM C759-98
Note: WITHDRAWN
Publication date standards: 10.2.1998
SKU: NS-14913
The number of pages: 17
Approximate weight : 51 g (0.11 lbs)
Country: American technical standard
Category: Technical standards ASTM

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Annotation of standard text ASTM C759-98 :

Keywords:

impurity content, isotopic composition, plutonium content, plutonium nitrate, ICS Number Code 27.120.30 (Fissile materials and nuclear fuel technology)

Additional information

1. Scope

1.1 These test methods cover procedures for the chemical, mass spectrometric, spectrochemical, nuclear, and radiochemical analysis of nuclear-grade plutonium nitrate solutions to determine compliance with specifications.

1.2 The analytical procedures appear in the following order:

Sections Plutonium by Controlled-Potential Coulometry 2 Plutonium by Amperometric Titration with Iron (II) 2 Free Acid by Titration in an Oxalate Solution 16 to 23 Free Acid by Iodate Precipitation- Potentiometric Titration Test Method 24 to 30 Uranium by Arsenazo I Spectrophotometric Test Method 31 to 41 Thorium by Thorin Spectrophotometric Test Method 42 to 50 Iron by 1,10-Phenanthroline Spectrophotometric Test Method 51 to 58 Chloride by Thiocyanate Spectrophotometric Test Method 59 to 66 Fluoride by Distillation-Spectrophotometric Test Method 67 to 74 Sulfate by Barium Sulfate Turbidimetric Test Method 75 to 82 Isotopic Composition by Mass Spectrometry 83 to 84 Americium-241 by Extraction and Gamma Counting 85 to 93 Americium-241 by Gamma Counting 94 to 102 Gamma-Emitting Fission Products, Uranium, and Thorium by Gamma-Ray Spectroscopy 103 to 110 Rare Earths by Copper Spark Spectrochemical Test Method 111 to 113 Tungsten, Niobium (Columbium), and Tantalum by Spectro-chemical Test Method 114 to 122 Sample Preparation for Spectrographic Analysis for General Impurities 123 to 126

1.3 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific safeguard and safety hazard statements, see Section 5.

2. Referenced Documents

C1415-24	Standard Test Method for 238Pu Isotopic Abundance by Alpha Spectrometry
E115-97	Standard Practice for Photographic Processing in Optical Emission Spectrographic Analysis (Withdrawn 2002)
E116-97	Standard Practice for Photographic Photometry in Spectrochemical Analysis (Withdrawn 2002)
C1432-23	Standard Test Method for Determination of Impurities in Plutonium: Acid Dissolution, Ion Exchange Matrix Separation, and Inductively Coupled Plasma-Atomic Emission Spectroscopic (ICP/AES) Analysis
D1193-24	Standard Specification for Reagent Water
E50-25	Standard Practices for Apparatus, Reagents, and Safety Considerations for Chemical Analysis of Metals, Ores, and Related Materials
C1128-23	Standard Guide for Preparation of Working Reference Materials for Use in Analysis of Nuclear Fuel Cycle Materials
C1156-18	Standard Guide for Establishing Calibration for a Measurement Method Used to Analyze Nuclear Fuel Cycle Materials
C1165-23	Standard Test Method for Determining Plutonium by Controlled-Potential Coulometry in H2SO4 at a Platinum Working Electrode
C1206-02	Standard Test Method for Plutonium by Iron (II)/Chromium (VI) Amperometric Titration
C1210-21	Standard Guide for Establishing a Measurement System Quality Control Program for Analytical Chemistry Laboratories Within Nuclear Industry
C1235-99	Standard Test Method for Plutonium by Titanium(III)/Cerium(IV) Titration (Withdrawn 2005)
C1268-23	Standard Test Method for Quantitative Determination of 241Am in Plutonium by Gamma-Ray Spectrometry
C1297-18	Standard Guide for Qualification of Laboratory Analysts for the Analysis of Nuclear Fuel Cycle Materials
C1307-21	Standard Test Method for Plutonium Assay by Plutonium (III) Diode Array Spectrophotometry
C697-24	Standard Test Methods for Chemical, Mass Spectrometric, and Spectrochemical Analysis of Nuclear-Grade Plutonium Dioxide Powders and Pellets
C852-09	Standard Guide for Design Criteria for Plutonium Gloveboxes
C1009-21	Standard Guide for Establishing and Maintaining a Quality Assurance Program for Analytical Laboratories Within the Nuclear Industry
C1068-21	Standard Guide for Qualification of Measurement Methods by a Laboratory Within the Nuclear Industry
C1108-23	Standard Test Method for Plutonium by Controlled-Potential Coulometry

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