ASTM D5412-93(2000)

Standard Test Method for Quantification of Complex Polycyclic Aromatic Hydrocarbon Mixtures or Petroleum Oils in Water

STANDARD published on 1.1.2000

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The information about the standard:

Designation standards: ASTM D5412-93(2000)
Note: WITHDRAWN
Publication date standards: 1.1.2000
SKU: NS-31071
The number of pages: 11
Approximate weight : 33 g (0.07 lbs)
Country: American technical standard
Category: Technical standards ASTM

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Annotation of standard text ASTM D5412-93(2000) :

Keywords:

creosotes, fluorescence, fuel oils, oil characterization, oil classification, oil quantification, PAH quantification, PAHs, petroleum oils, synchronous fluorescence, ultraviolet-visible fluorescence, ICS Number Code 13.060.50 (Examination of water for chemical substances)

Additional information

1. Scope

1.1 This test method covers a means for quantifying or characterizing total polycyclic aromatic hydrocarbons (PAHs) by fluorescence spectroscopy (Fl) for waterborne samples. The characterization step is for the purpose of finding an appropriate calibration standard with similiar emission and synchronous fluorescence spectra.

1.2 This test method is applicable to PAHs resulting from petroleum oils, fuel oils, creosotes, or industrial organic mixtures. Samples can be weathered or unweathered, but either the same material or appropriately characterized site-specific PAH or petroleum oil calibration standards with similar fluorescence spectra should be chosen. The degree of spectral similarity needed will depend on the desired level of quantification and on the required data quality objectives.

1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

2. Referenced Documents

D3325-90(2020)	Standard Practice for Preservation of Waterborne Oil Samples
D2777-21	Standard Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water
D1129-24	Standard Terminology Relating to Water
D1193-24	Standard Specification for Reagent Water
D3415-98(2024)	Standard Practice for Identification of Waterborne Oils
D3326-07(2024)	Standard Practice for Preparation of Samples for Identification of Waterborne Oils
E578-07(2021)	Standard Test Method for Linearity of Fluorescence Measuring Systems
E388-04(2023)	Standard Test Method for Wavelength Accuracy and Spectral Bandwidth of Fluorescence Spectrometers
E275-08(2022)	Standard Practice for Describing and Measuring Performance of Ultraviolet and Visible Spectrophotometers
E169-16(2022)	Standard Practices for General Techniques of Ultraviolet-Visible Quantitative Analysis
E131-10(2023)	Standard Terminology Relating to Molecular Spectroscopy
D4657-92(1998)	Standard Test Method for Polynuclear Aromatic Hydrocarbons in Water (Withdrawn 2005)
D4489-95(2024)	Standard Practices for Sampling of Waterborne Oils
D3650-93(1999)	Standard Test Method for Comparison of Waterborne Petroleum Oils By Fluorescence Analysis
E579-04(2023)	Standard Test Method for Limit of Detection of Fluorescence of Quinine Sulfate in Solution

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