ASTM D8001-16e1

Standard Test Method for Determination of Total Nitrogen, Total Kjeldahl Nitrogen by Calculation, and Total Phosphorus in Water, Wastewater by Ion Chromatography (Includes all amendments And changes 11/25/2024).

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STANDARD published on 15.7.2016

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The information about the standard:

Designation standards: ASTM D8001-16e1
Note: WITHDRAWN
Publication date standards: 15.7.2016
SKU: NS-652922
The number of pages: 11
Approximate weight : 33 g (0.07 lbs)
Country: American technical standard
Category: Technical standards ASTM

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The category - similar standards:

Examination of water for chemical substances

Annotation of standard text ASTM D8001-16e1 :

Keywords:

alkaline persulfate digestion, ion chromatography, nitrate, ortho-phosphate, phosphate, total Kjeldahl nitrogen, total nitrogen, total phosphate,, ICS Number Code 13.060.50 (Examination of water for chemical substances)

Additional information

Significance and Use

5.1 This test method allows the simultaneous determination of total nitrogen and total phosphorous from one sample digestion step.

5.2 This test method measures oxidized ammonia and organic nitrogen (as nitrate) and soluble nitrate simultaneously. By subtracting the nitrate + nitrite value from a non-digested sample gives a TKN:

When using this test method:

1.1 This test method is applicable for the analysis total nitrogen (organic nitrogen + ammonia-N + nitrate-N + nitrite-N) as nitrate and total phosphorus as orthophosphate in unfiltered water samples by alkaline persulfate digestion followed by ion chromatography (IC). 1.2 Total Kjeldahl nitrogen (TKN) is determined by the calculation. To determine TKN subtract the nitrate-N and nitrite-N in a digested sample from a non-digested sample (see Section 4, Summary of Test Method). 1.3 The limit of detection (LOD), limit of quantitation (LOQ), and reporting range in Table 1 are based on the two-step process for this test method: digestion and analytical step. Because the digestion step requires a sample dilution, the LOD and LOQ are higher than undigested samples. The reporting range, LOD, and LOQ can be modified and perhaps improved depending on several factors (see Section 6, Interferences). where:
A	=	the average method blank concentration,
	=	the student’s t-value for the single-tailed 99th percentile t statistic a standard deviation estimate with S_b	=	the sample standard deviation of the replicate blank analyses.

1.4 The method detection limits (MDL) are shown for reference. The digestion reagent contains background nitrate and results in higher detection limits. MDL will be shown after the interlaboratory study (ILS) is completed.

1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

2. Referenced Documents

D1193-06(2018)	Standard Specification for Reagent Water
D2777-21	Standard Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water
D4327-17	Standard Test Method for Anions in Water by Suppressed Ion Chromatography
D5847-22	Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
D5810-96(2021)	Standard Guide for Spiking into Aqueous Samples
D3856-11	Standard Guide for Management Systems in Laboratories Engaged in Analysis of Water
D1129-13(2020)e2	Standard Terminology Relating to Water (Includes all amendments and changes 2/14/2024).
D6299-23a	Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance (Includes all amendments and changes 12/12/2023).
D6792-23c	Standard Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories (Includes all amendments and changes 12/7/2023).

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