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Standard ASTM E1473-22 15.11.2022 preview

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ASTM E1473-22

Standard Test Methods for Chemical Analysis of Nickel, Cobalt, and High-Temperature Alloys

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STANDARD published on 15.11.2022

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The information about the standard:

Designation standards: ASTM E1473-22
Publication date standards: 15.11.2022
SKU: NS-1097767
The number of pages: 38
Approximate weight : 114 g (0.25 lbs)
Country: American technical standard
Category: Technical standards ASTM

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Nickel, chromium and their alloys

Annotation of standard text ASTM E1473-22 :

Keywords:
aluminum, chromium, cobalt, cobalt-base alloys, copper, high temperature alloys, iron, manganese, molybdenum, nickel, nickel-base alloys, niobium, silicon, tantalum, tin,, ICS Number Code 77.120.40 (Nickel, chromium and their alloys)

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Significance and Use

4.1?These test methods for the chemical analysis of metals and alloys are primarily intended as referee methods to test such materials for compliance with compositional specifications, particularly those under the jurisdiction of Committee B02 on Nonferrous Metals and Alloys. It is assumed that all who use these test methods will be trained analysts capable of performing common laboratory procedures skillfully and safely. It is expected that work will be performed in a properly equipped laboratory under appropriate quality control practices such as those described in Guide E882.

1. Scope

1.1?These test methods describe the chemical analysis of nickel, cobalt, and high-temperature alloys having chemical compositions within the following limits:

Element

Composition Range, %

Aluminum

0.005

7.00

Beryllium

0.001

0.05

Boron

0.001

1.00

Calcium

0.002

0.05

Carbon

0.001

1.10

Chromium

0.10

33.00

Cobalt

0.10

75.00

Copper

0.01

35.00

Iron

0.01

50.00

Lead

0.001

0.01

Magnesium

0.001

0.05

Manganese

0.01

3.0

Molybdenum

0.01

30.0

Niobium (Columbium)

0.01

6.0

Nickel

0.10

98.0

Nitrogen

0.001

0.20

Phosphorus

0.002

0.08

Sulfur

0.002

0.10

Silicon

0.01

5.00

Tantalum

0.005

1.00

Tin

0.002

0.10

Titanium

0.01

5.00

Tungsten

0.01

18.00

Vanadium

0.01

3.25

Zinc

0.001

0.01

Zirconium

0.01

2.50

1.2?The test methods in this standard are contained in the sections indicated as follows:

Aluminum, Total by the 8-Quinolinol Gravimetric Method
(0.20 % to 7.00 %)

53 to 60

Chromium by the Atomic Absorption Spectrometry Method
(0.018 % to 1.00 %)

91 to 100

Chromium by the Peroxydisulfate OxidationTitration Method
(0.10 % to 33.00 %)

101 to 109

Cobalt by the Ion-Exchange-Potentiometric Titration Method
(2 % to 75 %)

25 to 32

Cobalt by the Nitroso-R-Salt Spectrophotometric Method
(0.10 % to 5.0 %)

33 to 42

Copper by Neocuproine Spectrophotometric Method
(0.010 % to 10.00 %)

43 to 52

Iron by the Silver Reduction Titrimetric Method
(1.0 % to 50.0 %)

118 to 125

Manganese by the Metaperiodate Spectrophotometric Method
(0.05 % to 2.00 %)

8 to 17

Molybdenum by the Ion Exchange8-Hydroxyquinoline
Gravimetric Method (1.5 % to 30 %)

110 to 117

Molybdenum by the Thiocyanate Spectrophotometric Method
(0.01 % to 1.50 %)

79 to 90

Nickel by the Dimethylglyoxime Gravimetric Method
(0.1 % to 84.0 %)

61 to 68

Niobium by the Ion ExchangeCupferron Gravimetric Method
(0.5 % to 6.0 %)

126 to 133

Silicon by the Gravimetric Method (0.05 % to 5.00 %)

18 to 24

Tantalum by the Ion ExchangePyrogallol Spectrophotometric
Method (0.03 % to 1.0 %)

134 to 142

Tin by the Solvent Extraction-Atomic Absorption Spectrometry Method (0.002 % to 0.10 %)

69 to 78

1.3?Other test methods applicable to the analysis of nickel alloys that may be used in lieu of or in addition to this method are E1019, E1834, E1835, E1917, E1938, E2465, E2594, E2823.

1.4?Some of the composition ranges given in 1.1 are too broad to be covered by a single method, and therefore, these test methods contain multiple methods for some elements. The user must select the proper test method by matching the information given in the scope and interference sections of each test method with the composition of the alloy to be analyzed.

1.5?UnitsThe values stated in SI units are regarded as standard.

1.6?This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.7?This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

2. Referenced Documents

E1938-13(2018)	Standard Test Method for Determination of Titanium in Nickel Alloys by Diantipyrylmethane Spectrophotometry
E2465-23	Standard Test Method for Analysis of Ni-Base Alloys by Wavelength Dispersive X-Ray Fluorescence Spectrometry
E2594-20	Standard Test Method for Analysis of Nickel Alloys by Inductively Coupled Plasma Atomic Emission Spectrometry (Performance-Based)
E2823-17	Standard Test Method for Analysis of Nickel Alloys by Inductively Coupled Plasma Mass Spectrometry (Performance-Based)
ISO 5725	Precision of Test Methods--Determination of Repeatability and Reproducibility for Inter-Laboratory Tests
E1917-13(2018)	Standard Test Method for Determination of Phosphorus in Nickel, Ferronickel, and Nickel Alloys by Phosphovanadomolybdate Spectrophotometry
E173-93	Practice for Conducting Interlaboratory Studies of Methods for Chemical Analysis of Metals (Withdrawn 1997)
E350-23	Standard Test Methods for Chemical Analysis of Carbon Steel, Low-Alloy Steel, Silicon Electrical Steel, Ingot Iron, and Wrought Iron
E351-18	Standard Test Methods for Chemical Analysis of Cast Iron´All Types
E352-23	Standard Test Methods for Chemical Analysis of Tool Steels and Other Similar Medium- and High-Alloy Steels
E353-19e1	Standard Test Methods for Chemical Analysis of Stainless, Heat-Resisting, Maraging, and Other Similar Chromium-Nickel-Iron Alloys (Includes all amendments and changes 2/23/2022).
E354-21e1	Standard Test Methods for Chemical Analysis of High-Temperature, Electrical, Magnetic, and Other Similar Iron, Nickel, and Cobalt Alloys (Includes all amendments and changes 2/23/2022).
E882-10(2016)e1	Standard Guide for Accountability and Quality Control in the Chemical Analysis Laboratory (Includes all amendments and changes 10/27/2017).
E1601-19	Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method
E1834-18	Standard Test Method for Analysis of Nickel Alloys by Graphite Furnace Atomic Absorption Spectrometry
E1835-14(2022)	Standard Test Method for Analysis of Nickel Alloys by Flame Atomic Absorption Spectrometry
E1019-18	Standard Test Methods for Determination of Carbon, Sulfur, Nitrogen, and Oxygen in Steel, Iron, Nickel, and Cobalt Alloys by Various Combustion and Inert Gas Fusion Techniques
E60-11(2022)e1	Standard Practice for Analysis of Metals, Ores, and Related Materials by Spectrophotometry (Includes all amendments and changes 6/29/2022).
E135-23a	Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials (Includes all amendments and changes 7/17/2023).
D1193-06(2018)	Standard Specification for Reagent Water
E29-22	Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
E50-17	Standard Practices for Apparatus, Reagents, and Safety Considerations for Chemical Analysis of Metals, Ores, and Related Materials

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