Standard Test Methods for Kinetic Parameters by Differential Scanning Calorimetry Using Isothermal MethodsTranslate name
STANDARD published on 1.4.2018
Designation standards: ASTM E2070-13(2018)
Publication date standards: 1.4.2018
The number of pages: 12
Approximate weight : 36 g (0.08 lbs)
Country: American technical standard
Category: Technical standards ASTM
activation energy, accelerating reactions, Avrami equation, crystallization reactions, differential scanning calorimetry (DSC), frequency factor, kinetics, nth order reactions, pre-exponential factor, reactions, Sestak-Berggren equation, thermal analysis, thermoset cure,, ICS Number Code 17.200.10 (Heat. Calorimetry)
|Significance and Use|
6.1 These test methods are useful for research and development, quality assurance, regulatory compliance, and specification acceptance purposes.
6.2 The determination of the order of a chemical reaction or transformation at specific temperatures or time conditions is beyond the scope of these test methods.
6.3 The activation energy results obtained by these test methods may be compared with those obtained from Test Method for 1.1 Test Methods A, B, and C determine kinetic parameters for activation energy, pre-exponential factor and reaction order using differential scanning calorimetry from a series of isothermal experiments over a small ( ≈10 K) temperature range. Test Method A is applicable to low nth order reactions. Test Methods B and C are applicable to accelerating reactions such as thermoset curing or pyrotechnic reactions and crystallization transformations in the temperature range from 300 to 900 K (nominally 30 to 630°C). These test methods are applicable only to these types of exothermic reactions when the thermal curves do not exhibit shoulders, double peaks, discontinuities or shifts in baseline.
1.2 Test Methods D and E also determines the activation energy of a set of time-to-event and isothermal temperature data generated by this or other procedures
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 These test methods are similar but not equivalent to ISO DIS 11357, Part 5, and provides more information than the ISO standard.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
|2. Referenced Documents|
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