ASTM E2981-15

4.1 The COPVs covered in this guide consist of a metallic liner overwrapped with high-strength fibers embedded in polymeric matrix resin (typically a thermoset) (Fig. 1). Metallic liners may be spun-formed from a deep drawn/extruded monolithic blank or may be fabricated by welding formed components. Designers often seek to minimize the liner thickness in the interest of weight reduction. COPV liner materials used can be aluminum alloys, titanium alloys, nickel-chromium alloys, and stainless steels, impermeable polymer liner such as high density polyethylene, or integrated composite materials. Fiber materials can be carbon, aramid, glass, PBO, metals, or hybrids (two or more types of fibers). Matrix resins include epoxies, cyanate esters, polyurethanes, phenolic resins, polyimides (including bismaleimides), polyamides and other high performance polymers. Common bond line adhesives are FM-73, urethane, West 105, and Epon 862 with thicknesses ranging from 0.13 mm (0.005 in.) to 0.38 mm (0.015 in.). Metallic liner and composite overwrap materials requirements are found in ANSI/AIAA S-080 and ANSI/AIAA S-081, respectively.

1.1 This guide discusses current and potential nondestructive testing (NDT) procedures for finding indications of discontinuities and accumulated damage in the composite overwrap of filament wound pressure vessels, also known as composite overwrapped pressure vessels (COPVs). In general, these vessels have metallic liner thicknesses less than 2.3 mm (0.090 in.), and fiber loadings in the composite overwrap greater than 60 percent by weight. In COPVs, the composite overwrap thickness will be of the order of 2.0 mm (0.080 in.) for smaller vessels and up to 20 mm (0.80 in.) for larger ones.

1.2 This guide focuses on COPVs with nonload-sharing metallic liners used at ambient temperature, which most closely represents a Compressed Gas Association (CGA) Type III metal-lined composite tank. However, it also has relevance to 1.3 The vessels covered by this guide are used in aerospace applications; therefore, the inspection requirements for discontinuities and inspection points will in general be different and more stringent than for vessels used in non aerospace applications.

1.4 This guide applies to 1) low pressure COPVs used for storing aerospace media at maximum allowable working pressures (MAWPs) up to 3.5 MPa (500 psia) and volumes up to 2 m³ (70 ft³), and 2) high pressure COPVs used for storing compressed gases at MAWPs up to 70 MPa (10,000 psia) and volumes down to 8000 cm³ (500 in.³). Internal vacuum storage or exposure is not considered appropriate for any vessel size.

1.5 The composite overwraps under consideration include but are not limited to ones made from various polymer matrix resins (for example, epoxies, cyanate esters, polyurethanes, phenolic resins, polyimides (including bismaleimides), and polyamides) with continuous fiber reinforcement (for example, carbon, aramid, glass, or poly-(phenylenebenzobisoxazole) (PBO)). The metallic liners under consideration include but are not limited to aluminum alloys, titanium alloys, nickel-chromium alloys, and stainless steels.

1.6 This guide describes the application of established NDT methods; namely, Acoustic Emission (AE, Section 7), Eddy Current Testing (ECT, Section 8), Laser Shearography (Section 9), Radiologic Testing (RT, Section 10), Thermographic Testing (TT, Section 11), Ultrasonic Testing (UT, Section 12), and Visual Testing (VT, Section 13). These methods can be used by cognizant engineering organizations for detecting and evaluating flaws, defects, and accumulated damage in the composite overwrap of new and in-service COPVs.

1.7 All methods discussed in this guide (AE, ET, shearography, RT, TT, UT, and VT) are performed on the composite overwrap after overwrapping and structural cure. For NDT procedures for detecting discontinuities in thin-walled metallic liners in filament wound pressure vessels, or in the bare metallic liner before overwrapping; namely, AE, ET, laser profilometry, leak testing (LT), penetrant testing (PT), and RT; consult Guide E2982.

1.8 In the case of COPVs which are impact damage sensitive and require implementation of a damage control plan, emphasis is placed on NDT methods that are sensitive to detecting damage in the composite overwrap caused by impacts at energy levels and which may or may not leave any visible indication on the COPV composite surface.

1.9 This guide does not specify accept-reject criteria (subsection 4.9) to be used in procurement or used as a means for approving filament wound pressure vessels for service. Any acceptance criteria specified are given solely for purposes of refinement and further elaboration of the procedures described in this guide. Project or original equipment manufacturer (OEM) specific accept/reject criteria shall be used when available and take precedence over any acceptance criteria contained in this document. If no accept/reject criteria are available, any NDT method discussed in this guide that identifies broken fibers shall require disposition by the cognizant engineering organization.

1.10 This guide references both established ASTM methods that have a foundation of experience and that yield a numerical result, and newer procedures that have yet to be validated and are better categorized as qualitative guidelines and practices. The latter are included to promote research and later elaboration in this guide as methods of the former type.

1.11 To ensure proper use of the referenced standard documents, there are recognized NDT specialists that are certified according to industry and company NDT specifications. It is recommended that an NDT specialist be a part of any composite component design, quality assurance, in-service maintenance, or damage examination.

1.12 The values stated in SI units are to be regarded as standard. The English units given in parentheses are provided for information only.

1.13 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Some specific hazards statements are given in Section 7 on Hazards.