ASTM E354-93(2000)e1

Standard Test Methods for Chemical Analysis of High-Temperature, Electrical, Magnetic, and Other Similar Iron, Nickel, and Cobalt Alloys (Includes all amendments And changes 8/16/2017).

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Standard Test Methods for Chemical Analysis of High-Temperature, Electrical, Magnetic, and Other Similar Iron, Nickel, and Cobalt Alloys

STANDARD published on 1.1.2000

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The information about the standard:

Designation standards: ASTM E354-93(2000)e1
Note: WITHDRAWN
Publication date standards: 1.1.2000
SKU: NS-46532
The number of pages: 28
Approximate weight : 84 g (0.19 lbs)
Country: American technical standard
Category: Technical standards ASTM

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Annotation of standard text ASTM E354-93(2000)e1 :

Keywords:
aluminum, chromium, cobalt, cobalt alloys, combustion analysis, copper, high temperature alloys, induction furnace, infrared absorption, iron, manganese, magnetic alloys, molybdenum, nickel, nickel alloys, phosphorus, silicon, sulfur, tin, total carbon, ICS Number Code 77.140.40 (Steels with special magnetic properties)

Additional information

1. Scope

1.1 These test methods cover the chemical analysis of high-temperature, electrical, magnetic, and other similar iron, nickel, and cobalt alloys having chemical compositions within the following limits:

Element	Concentration Range, %

Aluminum	0.005	to	18.00
Beryllium	0.001	to	0.05
Boron	0.001	to	1.00
Calcium	0.002	to	0.05
Carbon	0.001	to	1.10
Chromium	0.10	to	33.00
Cobalt	0.10	to	75.00
Columbium (Niobium)	0.01	to	6.0
Copper	0.01	to	10.00
Iron	0.01	to	85.00
Magnesium	0.001	to	0.05
Manganese	0.01	to	3.0
Molybdenum	0.01	to	30.0
Nickel	0.10	to	84.0
Nitrogen	0.001	to	0.20
Phosphorus	0.002	to	0.08
Silicon	0.01	to	5.00
Sulfur	0.002	to	0.10
Tantalum	0.005	to	10.0
Titanium	0.01	to	5.00
Tungsten	0.01	to	18.00
Vanadium	0.01	to	3.25
Zirconium	0.01	to	2.50

1.2 The test methods in this standard are contained in the sections indicated below:

	Sections

Aluminum, Total, by the 8-Quinolinol Gravimetric Method (0.20 to7.00 %)	100
Carbon,Total, by the Combustion-Thermal Conductivity Method	¹^a
Carbon, Total, by the Combustion Gravimetric Method (0.05 to1.10 %)	79
Chromium by the Atomic Absorption Method (0.006 to 1.00 %)	165
Chromium by the Peroxydisulfate Oxidation-Titration Method(0.10 to 33.00 %)	175
Chromium by the Peroxydisulfate-Oxidation Titrimetric Method	¹^b
Cobalt by the Ion-Exchange-Potentiometric Titration Method (2 to75 %)	53
Cobalt by the Nitroso-R-Salt Photometric Method (0.10 to 5.0 %)	61
Copper by Neocuproine Photometric Method (0.01 to 10.00 %)	90
Copper by the Sulfide Precipitation-Electrodeposition GravimetricMethod (0.01 to 10.00 %)	71
Iron by the Silver ReductionTitrimetric Method (1.0 to 50.0 %)	192
Manganese by the Periodate Photometric Method (0.05 to 2.00 %)
Molybdenum by the Ion Exchange-8-Hydroxyquinoline Gravi-metric Method (1.5 to 30 %)	184
Molybdenum by the Photometric Method (0.01 to 1.50 %)	153
Nickel by the Dimethylglyoxime Gravimetric Method (0.1 to84.0 %)	135
Phosphorus by the Molybdenum Blue Photometric Method (0.002to 0.08 %)	18
Silicon by the Gravimetric Method (0.05 to 5.00 %)	46
Sulfur by the Gravimetric Method	¹ ^c
Sulfur by the Combustion-Iodate Titration Method (0.005 to0.1 %)	37
Sulfur by the Chromatographic Gravimetric Method	^1b
Tin by the Solvent Extraction-Atomic Absorption Method (0.002to 0.10 %)	143

1.3 Methods for the determination of several elements not included in this standard can be found in Test Methods E30 and Test Methods E1019.

1.4 Some of the concentration ranges given in 1.1 are too broad to be covered by a single method and therefore this standard contains multiple methods for some elements. The user must select the proper method by matching the information given in the Scope and Interference sections of each method with the composition of the alloy to be analyzed.

1.5 The values stated in SI units are to be regarded as standard. In some cases, exceptions allowed in Practice E380 are also used.

1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific hazards statements are given in Section 5 and in special "Warning" paragraphs throughout these test methods.

2. Referenced Documents

E350-23	Standard Test Methods for Chemical Analysis of Carbon Steel, Low-Alloy Steel, Silicon Electrical Steel, Ingot Iron, and Wrought Iron
D1193-06(2018)	Standard Specification for Reagent Water
E29-22	Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
E50-17	Standard Practices for Apparatus, Reagents, and Safety Considerations for Chemical Analysis of Metals, Ores, and Related Materials
E60-11(2022)e1	Standard Practice for Analysis of Metals, Ores, and Related Materials by Spectrophotometry (Includes all amendments and changes 6/29/2022).
E135-23a	Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials (Includes all amendments and changes 7/17/2023).
E173-93	Practice for Conducting Interlaboratory Studies of Methods for Chemical Analysis of Metals (Withdrawn 1997)
E351-18	Standard Test Methods for Chemical Analysis of Cast Iron´All Types
E353-19e1	Standard Test Methods for Chemical Analysis of Stainless, Heat-Resisting, Maraging, and Other Similar Chromium-Nickel-Iron Alloys (Includes all amendments and changes 2/23/2022).
E882-10(2016)e1	Standard Guide for Accountability and Quality Control in the Chemical Analysis Laboratory (Includes all amendments and changes 10/27/2017).
E1019-18	Standard Test Methods for Determination of Carbon, Sulfur, Nitrogen, and Oxygen in Steel, Iron, Nickel, and Cobalt Alloys by Various Combustion and Inert Gas Fusion Techniques
E1601-19	Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method
E1806-23	Standard Practice for Sampling Steel and Iron for Determination of Chemical Composition
ISO?5725	Precision of Test Methods--Determination of Repeatability and Reproducibility for Inter-Laboratory Tests Available from American National Standards Institute (ANSI), 25 W. 43rd St., 4th Floor, New York, NY 10036, http://www.ansi.org.
E352-23	Standard Test Methods for Chemical Analysis of Tool Steels and Other Similar Medium- and High-Alloy Steels

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