ČSN EN 16215 (467013)

Animal feeding stuffs: Methods of sampling and analysis - Determination of dioxins and dioxin-like PCBs by GC/HRMS and of indicator PCBs by GC/HRMS

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STANDARD published on 1.7.2020


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The information about the standard:

Designation standards: ČSN EN 16215
Classification mark: 467013
Catalog number: 509969
Publication date standards: 1.7.2020
SKU: NS-996309
The number of pages: 60
Approximate weight : 180 g (0.40 lbs)
Country: Czech technical standard
Category: Technical standards ČSN

The category - similar standards:

Animal feeding stuffs

Annotation of standard text ČSN EN 16215 (467013):

This document is applicable to the determination of polychlorinated dibenzo-p-dioxins (PCDDs), polychlorinated dibenzofurans (PCDFs), (together termed ´dioxins´ (PCDD/Fs)) and dioxin-like PCBs and non-dioxin-like PCBs (dl-PCBs and ndl-PCBs) in animal feeding stuffs. Collaborative studies have been carried out. The method is suitable for the determination of dioxins, dl-PCBs and ndl-PCBs at the appropriate MRL in compound feed and ingredients e.g. oil, mineral clay. The method is applicable to samples containing trace level amounts of one or more dioxins, dioxin-like PCBs and non-dioxin-likePCBs. The limit of quantification (LOQ) is - 0,05 pg/g (OCDD/F = 0,1 pg/g) for the relevant individual congeners of dioxins/furans, - 0,05 pg/g for non-ortho PCBs, - 10 pg/g for mono-ortho PCBs, and - 100 pg/g for non-dioxin-like-PCBs. For determination of dioxins and dioxin-like PCBs, the procedure can be used as confirmatory method as defined by Commission Regulation (EC) No 152/2009 for dioxins and dl-PCB in feed [1]. Confirmatory methods as described in this standard are high-resolution gas chromatography/high resolution mass spectrometry (HRGC/HRMS) methods. If only the analysis of non-dioxin-like PCBs is required, a GC-LRMS method can be used (e.g. EN 15741 [2]) provided that appropriate analytical performance criteria are met in the relevant range for the matrix of interest

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