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ČSN EN 17425 (560149)
Foodstuffs - Determination of ergot alkaloids in cereals and cereal products by dSPE clean-up and HPLC-MS/MS
Translate name
STANDARD published on 1.10.2021
The information about the standard:
Designation standards: ČSN EN 17425
Classification mark: 560149
Catalog number: 512738
Publication date standards: 1.10.2021
SKU: NS-1036852
The number of pages: 48
Approximate weight : 144 g (0.32 lbs)
Country: Czech technical standard
Category: Technical standards ČSN
The category - similar standards:
General methods of tests and analysis for food productsCereals, pulses and derived products
Annotation of standard text ČSN EN 17425 (560149):
This document describes a method for the determination of the sum of six ergot alkaloids (ergocornine, ergometrine, ergocristine, ergotamine, ergosine and ergocryptine) and their -inine epimer pairs by liquid chromatography coupled with tandem mass spectrometry (LC-MS/MS) after clean-up by dispersive solid phase extraction (dSPE). The method has been validated in the range 13,2 µg/kg to 168 µg/kg for the sum of the twelve ergot alkaloids, in rye flour, rye bread and cereal products (breakfast cereal, infant breakfast cereal, and crispbread) that contained rye as an ingredient, as well as seeded wholemeal flour and a barley and rye flour mixture. Method performance was satisfactory in the range 24,1 µg/kg to 168 µg/kg, however at lower concentrations RSDR values were greater than 44 %, and HorRat values exceeded 2,0, indicating the method may not be fully suitable at concentrations below 24 µg/kg for sum of ergot alkaloids, although it is suitable for screening at these concentrations
Preview of the standard ČSN EN 17425 (560149)
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